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Beilstein J. Org. Chem. 2019, 15, 1331–1338, doi:10.3762/bjoc.15.132
Graphical Abstract
Figure 1: Interactions of a pair of dipolar rotors in different orientations. The axes of the rotors are para...
Figure 2: Structures of molecular dipolar rotors/linker molecules 1–5.
Scheme 1: General synthetic strategy to prepare the dipolar rotors 1–5.
Scheme 2: Synthesis of 3,3'-(2,3-difluoro-1,4-phenylene)dipropiolic acid (1) starting with diiodination of 1,...
Scheme 3: Synthesis of 3,3'-(5,6-Difluoro-2,1,3-benzothiadiazol-4,7-diyl)dipropiolic acid (2) and 3,3'-(5,6-D...
Scheme 4: Synthesis of 3,3'-(5,6-dicyano-1,3-benzodioxole-4,7-diyl)dipropiolic acid (4) and 3,3'-(6,7-dicyano...